Inspired by data sent from NASA robots on Mars, Ronald Peterson, professor of geology at Queen’s Univ. in Kingston, Canada, has observed a new mineral species on Earth, and predicts that it also exists on Mars. The mineral, meridianiite (MgSO411H2O), was named in acknowledgement of the cratered plain of Meridiani Planum on Mars, where one of the NASA robots is operating.
The search for the new mineral began with data from two NASA Mars Exploration Rovers (MER). MER images of euhedral molds in sedimentary rock, together with data showing magnesium rich soil, led Peterson to suspect that the observed crystal molds could be formed by MgSO411H2O crystals precipitated from a MgSO4 rich solution. Such crystals were only known to form synthetically on Earth. With this information, Peterson set out to find sites where the material could occur naturally.
Frozen ponds in British Columbia, which were once mined for magnesium sulfate, were identified as a potential location. Here, Peterson found a tree trunk protruding from the ice that had drawn up the pond solution and allowed it to evaporate in air, at colder temperatures than below the ice. This resulted in the deposition of off-white crystals, which later proved to be meridianiite.
Integral to Peterson’s work was an instrument from PANalytical , the X’Pert PRO X-ray diffractometer. Designed for fast and portable detection processes, it is designed with a mounting method that enables optics and stages to be reconfigured in minutes.
Peterson and his colleagues made their discovery at a frozen pond in British Columbia, Canada. From collection to analysis, mineral samples had to be maintained at the sub-zero temperatures at which they were found. Even a small temperature rise would have altered the material completely.
Peterson says the combination of PANalytical’s X’Celerator detector and the PreFIX sample stage system was what made a quick analysis of the mineral possible.
“The Anton Paar chamber with the high thermal mass was also important, to ensure the sample did not warm up too much before we could measure the diffraction pattern. I loaded the sample into the stage that was already cold from being outside, then quickly took it into the lab, rapidly mounted the stage using the PreFIX system, and did a fast scan,” says Peterson.
The powder diffraction data, chemical analysis and physical properties were submitted to the International Mineralogical Association who approved the material as a valid new mineral species, and accepted the name meridianiite. It is expected that Meridianiite is the magnesium sulfate mineral in equilibrium with ice in the polar caps of Mars.
